Artificial joint made from zirconia-alumina composite ceramic
A technology of composite ceramics and artificial joints, applied in hip joints, internal bone synthesis, joint implants, etc.
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Embodiment 1
[0037] (Example 1 and Comparative Examples 1-3)
[0038] Tetragonal zirconia powder (amount of tetragonal zirconia: 98% by volume), which contained 10 mol% of ceria, 0.05 mol% of titania and 0.05 mol% of calcium oxide relative to the total amount of zirconia, was compared with The alumina powder was mixed with 30% by volume of the total volume of the zirconia-alumina composite ceramics to obtain a mixed powder. After the mixed powder was molded by unidirectional pressing and isostatic pressing to obtain a compact with a desired shape, the compact was pressurelessly sintered at 1400°C for 5 hours under atmospheric pressure. Thus, the zirconia-alumina composite ceramic of Example 1 having an average particle diameter of 0.22 μm was obtained. In order to evaluate the wear resistance and friction coefficient of this composite ceramic, a dial wear test was performed with distilled water as lubricant.
[0039] As a comparative example, an alumina sintered body having an average pa...
Embodiment 2-5
[0063] (embodiment 2-5 and comparative example 4)
[0064] Tetragonal zirconia powder (amount of tetragonal zirconia: 98% by volume), which contains 10 mol% of ceria and 0.05 mol% of titania relative to the total amount of zirconia, was compounded with zirconia-alumina 35% by volume of the total volume of the ceramics was mixed with alumina powder to obtain a mixed powder. After the mixed powder was molded by unidirectional pressing and isostatic pressing to obtain a compact of desired shape, as shown in Table 2, the compact was sintered without pressure for 5 hours at different temperatures and atmospheric pressure. Thus, the zirconia-alumina composite ceramics of Examples 2-5 and Comparative Example 4 were obtained. In Comparative Example 4, since the sintering temperature was 1600° C., the average grain size of the obtained composite ceramic was 1.65 μm, which was inconsistent with the composite ceramic of the present invention. After performing heat treatment and polishi...
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Abstract
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