The invention relates to a method for back extraction of amine 
molybdenum-containing organic phase. The method adopts 
single stage back extraction or multi-stage back current back extraction, the amine 
molybdenum-containing organic phase comprises the following components by concentration: 1-20% of amine, 1-30 g / L of 
molybdenum, and the balance a phase improver and a 
diluent. The method comprisesthe following steps that 1, a back extraction agent is prepared, the back extraction agent is 
mixed solution of 
ammonia and 
hydrogen peroxide, the 
ammonia concentration range is 5-28%, the 
hydrogen peroxide addition is 1-15% of the 
ammonia addition, and the concentration range of the 
hydrogen peroxide is 10-50%; 2, the back extraction agent prepared by the step one and the amine containing-molybdenum organic phase are subjected to mixing and back extraction, the 
flow ratio of the organic phase to a water phase is 2:1-50:1, the back extraction time is 1-10 min, the back extraction temperature is 10-40 DEG C, and the 
contact phase ratio between the organic phase and the water phase is 4:1-1:4; and 3, and the 
mixed phase obtained in the step two is separated to obtain the containing-molybdenum back extraction fluid and a stripped organic phase. By means of the method, the interfacial 
dirt produced in the back extraction process of the amine containing-molybdenum organic phase can be reduced by more than 50%.