The invention relates to a ferronickel 
hydroxide / reduction-oxidation 
graphene electrochemical 
oxygen evolution catalyst with 
nickel foam as a carrier and a preparation method of the ferronickel 
hydroxide / reduction-oxidation 
graphene electrochemical 
oxygen evolution catalyst. The 
nickel foam is used as the carrier of the catalyst, 
ferric hydroxide, 
nickel hydroxide or a compound of the 
ferric hydroxide and the nickel hydroxide is used as the 
active component of the catalyst, and reduction-oxidation 
graphene is used as the conductive material of the catalyst. The catalyst is prepared through a 
water heating and impregnation method. Firstly, the nickel foam is subjected to ultrasonic cleaning and 
drying; then, a certain amount of 
nickel salt and a certain amount of 
urea are weighed, dissolvedin deionized water and stirred to be evenly mixed at the 
room temperature; then, oxidized graphene is added, ultrasonic treatment is conducted, and evenly-dispersed mixed liquor is obtained; the nickel foam and the mixed liquor are transferred into a 
water heating kettle and react for 12 h to 24 h at the temperature being 120-200 DEG C; the nickel foam subjected to reaction is cleaned and dried;and finally, after the nickel foam is soaked in an iron 
salt solution with the concentration 
ranging from 5 mmol / L to 30 mmol / L for 0 h to 48 h, cleaning and 
drying are conducted, and the ferronickelhydroxide / reduction-oxidation graphene electrochemical 
oxygen evolution catalyst with the nickel foam as the carrier is obtained. The catalyst is good in 
catalysis activity and high in stability; andthe preparation method is simple and controllable, and industrial popularization is facilitated.