41 results about "Monobutyrin" patented technology

The invention relates to a composite feed additive for restoring baby pig intestine mucosal injury, belonging to the technical field of feed additives for baby pigs. The feed additive comprises 0.1-0.2 part of glutamine, 0.01-0.1 part of butyrin, 0.01-0.1 part of yeast nucleic acid, 0.02-0.2 part of threonine, 0.03-0.3 part of origanum oil, 0.03-0.3 part of chitooligosaccharide, 0.1-0.5 part of active dry yeast, 0.1-0.5 part of Bacillus subtilis, 0.11-0.3 part of vitamin and 5-7.5 parts of carrier. On the basis of the basic principles of baby pig intestinal tract nutrition, intestinal tract immunity and intestinal tract microecology, the invention can effectively restore baby pig intestine mucosal injury, accelerate the growth of baby pigs, and promote the health and immunity of the baby pig intestinal tract, thereby enhancing the survival rate and growth rate of the baby pigs.

The invention discloses a preparation method for a glycerol tributyrate microcapsule. The glycerol tributyrate microcapsule is prepared from the following raw materials: 100 parts of fatty acid, 50-100 parts of glycerol tributyrate, 1-10 parts of an emulsifier and 13-15 parts of calcium hydroxide. The preparation method comprises the following steps: mixing glycerol tributyrate, fatty acid and the emulsifier, heating, melting, and uniformly stirring in warm water with the temperature of 80+ / -5 DEG C to form emulsion; dissolving calcium hydroxide in water to prepare 10-20% of lime emulsion; mixing and stirring the emulsions obtained in the previous two steps and reacting to generate solid particles; filtering out the moisture and drying a filter cake to form the finished glycerol tributyrate microcapsule which freely flows at the room temperature. The preparation method has the advantages of low production cost, simple process, cheap equipment and favorability for industrialized production; the obtained finished solid particle product with the flowing property is relatively convenient when being used as an animal feed additive.

Belonging to the technical field of grease microcapsulation, the invention discloses a tributyrin microcapsule with maltodextrin and cyclodextrin as the wall material. The preparation process includes: adding maltodextrin and cyclodextrin into distilled water, conducting water bath heating at 50-80DEG C, and mixing the substances evenly, then adding tributyrin and an emulsifying agent, and fully stirring the substances evenly; and carrying out shearing, homogenizing and spray drying on the obtained mixture so as obtain a tributyrin microcapsule powder product. The method adopted by the invention has the characteristics of simple process and convenient operation. The prepared tributyrin microcapsule powder has the characteristics of small peculiar smell, and good stability and solubility, obviously improves the defects of peculiar smell, insolubility in water, poor fluidity and the like in tributyrin, and expands the application of tributyrin.

The invention discloses a method for clathrating tributyrin by an enzyme method, and belongs to the technical field of grease microencapsulation. According to the method, cyclodextrin synthesized by the enzyme method and tributyrin clathrated by cyclodextrin are combined. The method comprises the step of preparing the cyclodextrin by the enzyme method using CGT enzymes; the tributyrin is added inthe preparation process; after the reaction, Tween is added; and homogenizing and spray drying are performed. The effect of the finally obtained tributyrin powder is much better than the single cyclodextrin clathration effect. The method provided by the invention has the advantages that the process is simple; the cost is low; the operation is convenient; non-toxic harmless and pollution-free effects are achieved in the reaction process; no toxic reagent is remained; the clathration effect is obvious; and the better utilization of a nutritive additive of the tributyrin in the practical production is facilitated.

The invention relates to a synthetic method of tributyrin and application of tributyrin in feeds. The synthetic method comprises the steps of directly synthesizing tributyrin from butyric acid and glycerin in the absence of a solvent at a high temperature by virtue of a liquid catalyst, separating tributyrin from unreacted raw materials by virtue of a rectifying column through a high vacuum distillation method, collecting a corresponding fraction, namely tributyrin, and detecting the content of a distillation with a content above 98%(w / w) by virtue of a high performance liquid chromatography for reuse. According to the application, tributyrin produced by virtue of a process disclosed by the invention is used for preparing a feed additive capable of promoting the growth of economic animals and increasing the feed conversion rate, and the actual adding amount of the additive is 1000ppm-2000ppm; and compared with tributyrin produced by virtue of other processes in the market, the adding amount can be reduced.

The invention discloses a method of utilizing a Tween emulsifier to prepare microcapsule tributyrin and belongs to the technical field of oil microencapsulation. In the method, by taking cyclodextrin,dextrin and the like obtained after tributyrin is acted on starch or maltodextrin by using enzyme as wall materials, the wall materials are embedded with Tween as an emulsifier to prepare microcapsule tributyrin powder, peculiar smell of the tributyrin is removed, the stability and the solubility of the tributyrin are improved, and the method has an important significance to wide application of the tributyrin in the aspects of livestock feeds and breeding industry.

The invention provides an oplegnathus punctatus multi-functional composite feed and a preparation method thereof. The multi-functional composite feed comprises 25-30 parts of fish meal, 10-15 parts ofbroad bean powder, 10-20 parts of dextrin, 10-15 parts of cellulose, 2-3 parts of fish oil, 0.5-1 part of soybean lecithin, 1-2 parts of a mineral mixture, 0.3-0.5 part of a vitamin mixture, 0.1-0.2part of choline chloride, 0.1-0.5 part of calcium dihydrogen phosphate, 0.01-0.05 part of a tributyrin mixture and 0.01-0.03 part of a compound enzyme preparation, wherein the tributyrin mixture comprises 1-2 parts of butyrin, 1-3 parts of dibutyrin, 3-5 parts of tributyrin, 1-2 parts of vitamin C-phosphate ester and 1-3 parts of mannan oligosaccharides. The multi-functional feed can strengthen the immunomodulation of intestines of fish, can increase the growth speed, and can improve the growing performance, so that the fish muscle is tight in grains, and the fish is elastic and good in chewiness.

The invention discloses a pet beverage containing functional fatty acids and a preparation method of the pet beverage. Each 500ml of the pet beverage containing functional fatty acids comprises the following raw materials components of 1-10g of medium chain triglyceride, 1-10g of concentrated linolein, 0.1-1g of glycerol monolaurate, 0.2-2g of tributyrin, 0.1-1g of a composite emulsifying agent, 2-20g of a carrier and 0.005-0.05g of a composite antioxidant. The pet beverage containing functional fatty acids is used for balanced supplementing of fatty acids in bodies of pets, can effectively reduce cholesterol level in the bodies of the pets, and solves the problems that a conventional pet beverage is single in functions and poor in balance of nutrients. The preparation method of the pet beverage containing functional fatty acids adopts a microcapsule packing technique, so that the functional fatty acids are coated with the carrier, the stability and the solubility of the functional fatty acids in the pet beverage can be greatly improved, and efficient absorption of nutrient substances in the pet beverage by pets can be facilitated.

The invention relates to a method for compartment analysis of ferulic acid glycerol monobutyralte through the high performance liquid chromatography, comprising the following: firstly, a step of pretreatment, during which, ferulic acids and absolute ethyl alcohols generate reflux heating reaction under the catalysis of thionyl chlorides and are dissolved in aether and then ferulic acid methyl ethyl oxalate is obtained after extraction through sodium bicarbonate; under the temperature of between 30 and 50 DEG C, tertiary butyl alcohol is used as reaction medium and the ferulic acid glycerol monobutyralte is obtained through oscillating reaction of the ferulic acid methyl ethyl oxalate, glycerol monobutyralte and Novozym435 lipase in an air bath; the ferulic acid glycerol monobutyralte is dissolved in methanol, filtered and then diluted by HPLC-level methanol; secondly, a step of compartment analysis, which is to adopt a chromatographic column (Ph-3 column Inertsil, IDx250mm) with a column temperature of ambient temperature. A solid phase adopts silica gel filler and the ultraviolet detection wavelength is between 280 and 325 nanometers; a moving phase is gradient mixing of methanol and water; the sample feeding quantity is 5 mu L and the flow speed is 1mL / min. The method selects filler of the chromatographic column and the special ultraviolet scanning wavelength according to the characteristics of materials to be comparted, is quick, high-efficient and accurate and is convenient for industrial analysis and application.

The invention discloses a feed additive for enhancing the anti-stress ability of breeding ducks in the egg laying period and a preparation method of the feed additive. The additive comprises the following raw materials in percentage by weight: 3-5 parts of isochlorogenic acid, 1-3 parts of tributyrin, 2-4 parts of acetylglucosamine benzoate and 6-9 parts of puffed chickpea powder. The additive further comprises 1-3 parts of hyperforin perforatum and 1-3 parts of bile acid. The preparation method comprises the following steps: preparing a hyperforin perforatum extract: adding water twice for extraction, combining the two extracting solutions, concentrating to obtain paste, and drying to obtain the hyperforin perforatum extract; mixing and granulating to obtain granular products: wherein the variable coefficient of the mixing uniformity is less than or equal to 4%; sequentially spraying a tributyrin solution and an acetylglucosamine benzoate solution on the granular product; and drying. When the additive is added into the breeding duck feed, the physique, the resistance, the adaptive capacity to change of external factors such as feed changing and illumination increasing of the breeding ducks and the anti-stress capacity after egg laying can be effectively enhanced, and the overall economic benefit of duck breeding is improved.

The invention belongs to the technical field of preparation of glyceryl monobutyrate, and discloses a preparation process of glyceryl monobutyrate and a magnetic solid catalyst, the magnetic solid catalyst comprises: a carrier composed of Fe3O4 magnetic nanoparticles; the dispersed modification layer is formed by coating the carrier with polyacrylic acid; the porous composite layer is formed by crystallizing activated carbon, silicon dioxide and concentrated sulfuric acid and is attached to the outside of the dispersion modification layer, and sulfonic acid groups are distributed in pore channels of the porous composite layer; in conclusion, the magnetic material is introduced into the solid acid catalyst, so that the solid acid catalyst has certain magnetism and reaction stability under the condition of keeping relatively high catalytic activity; and the magnetic material carrier is coated with polyacrylic acid, so that the agglomeration phenomenon of nanoparticles of the magnetic material is effectively avoided, and the magnetic solid catalyst can effectively form uniform catalysis in the esterification reaction.

The invention discloses a synthesis method and application of high-purity monobutyric acid glyceride. The method comprises the following steps: (1) conducting esterification reaction of butyric acid and glycerin; (2) reducing the temperature of the system to below 60 DEG C, adding water 0.2-5 times of the total product weight, then obtaining a reaction mixture, adding lipases, and conducting stirring for hydrolysis reaction, so as to reduce the proportion of dibutyrate glycerol ester to 5-15% of the total ester; and the lipases are Novozym435, TL-100L, and PL20000; and (3) removing the lipasesfrom the reactant, and obtaining the high-purity monobutyric acid glyceride by molecular distillation. According to the present invention, the synthesis of high-purity monobutyric acid glyceride, andthe monobutyric acid glyceride is applied in preparing feed additives.

The invention relates to tributyrin microcapsule powder and a preparation method thereof, and is characterized in that the tributyrin microcapsule powder comprises the following components by weight: 40-55% of a core material, 45-55% of a wall material, 0.2-10% of an auxiliary wall material, 0.1-1% of an emulsifier, and 0.2-1% of a flavoring agent. The invention also discloses a preparation method of the tributyrin microcapsule powder. When the high-oil-loading microcapsule powder is prepared, the surface grease rate of the microcapsule powder can be remarkably reduced, the bitter taste and peculiar smell of tributyrin are effectively shielded, and the prepared product is moderate in taste, free of peculiar smell and good in market value.

The present invention refers to the use of a glycerol ester composition of at least one short chain fatty acid for preventing and / or alleviating necrotic enteritis in the gastric tract of galloanserans. The glycerol ester composition comprises at least 75% by weight of glyceryl tributyrate, below 25% by weight of glyceryl dibutyrate and below 8% by weight of glyceryl monobutyrate. The present invention also refers to the use of said composition for modulating the gut flora of galloanserans.

The invention relates to a butyrin complex for livestock and a preparation method and application of the butyrin complex. The butyrin complex for livestock consists of the following components in parts by weight: 100-300 parts of glycerol monobutyrate, 100-300 parts of glycerol polybutyrate, 50-150 parts of radix codonopsis pilosulae, 50-150 parts of poria, 50-150 parts of fried atractylodes macrocephala, 50-150 parts of Chinese yams, 50-100 parts of white hyacinth beans, 30-70 parts of fructus amomi, 50-150 parts of viable organisms of bifidobacterium, 50-250 parts of viable organisms of bacillus subtilis, 50-150 parts of viable organisms of lactobacillus and 100-200 parts of selenium yeast. The preparation method of the butyrin complex for livestock comprises the following steps: grinding the traditional Chinese medicines into powder, performing microorganism fermentation drying, performing superfine wall breaking crushing, and mixing materials. The butyrin complex for livestock, which is provided by the invention, is applied to livestock feeding, has the effects of improving the body immunity of animals and inhibiting reproduction of harmful bacteria, is capable of greatly increasing the laying rate and fertility rate, is free of toxic or side effect and is safe and reliable.

The invention belongs to the field of medicament preparing and particularly relates to norisoboldine self-microemulsion preparation and a preparing method thereof. The method includes: adding norisoboldine into anhydrous ethanol, adding tributyrin and emulsifier EL-40 after 37-DEG C ultrasonic dissolving saturation, and well mixing in a vortex manner to prepare the norisoboldine self-microemulsion preparation, wherein the volume fraction of the tributyrin in the self-microemulsion preparation is 22.5%; the volume ratio of the emulsifier to the anhydrous ethanol is 3:1. The norisoboldine self-microemulsion preparation prepared by the method is clear and transparent liquid and stable in property and forms O / W type light blue microemulsion when meeting water, the self-emulsifying rate of the norisoboldine self-microemulsion preparation is 28.3s, the particle size of the norisoboldine self-microemulsion preparation is 14.73 nanometers, the Zeta potential of the norisoboldine self-microemulsion preparation is 0.7mV, and the drug loading capacity of the norisoboldine self-microemulsion preparation is 14.8676mg / mL.

The present application provides an emulsion composition. The composition comprises butyrate, butyrin, a butyrin derivative or a mixture thereof, and / or glycerol laurate, a glycerol laurate derivativeor a mixtures thereof, where the pH value of the emulsion composition is 2-6. The invention further provides a preparation method of the emulsion composition and application of the emulsion composition in animal feeding.

The invention relates to the technical field of feed additives and relates to a fat function mixture for replacing an antibiotic growth promoting agent for livestock and a preparation method of the fat function mixture. The fat function mixture comprises the following components in parts by mass: 10-30 parts of clostridium butyricum, 20-45 parts of butyrin, 5-25 parts of short chain fatty acid, 5-20 parts of medium carbon chain fatty acid monoglyceride, 5-20 parts of an electrolyte, 1-12 parts of plant essential oil, 1-11 parts of an organic acid and 35-65 parts of a carrier. The preparation method of the fat function mixture for replacing the antibiotic growth promoting agent for livestock comprises the following steps: S1, mixing the plant essential oil, the butyrin, the short chain fatty acid and the medium carbon chain fatty acid monoglyceride so as to obtain a premixture; S2, mixing the electrolyte and the organic acid with the premixture so as to obtain a primary mixture; S3, homogenizing and emulsifying the primary mixture, and spraying the mixture to the carrier so as to obtain a medium mixture; and S4, uniformly mixing the medium mixture with the clostridium butyricum, soas to obtain the fat function mixture for replacing the antibiotic growth promoting agent for livestock. The fat function mixture has effects that the antibiotic growth promoting agent is replaced, and growth of chickens for meat can be well promoted.

The invention belongs to the technical field of substance content determination. The invention provides a method for determining the content of tributyrin, which comprises the following steps: mixing a tributyrin standard substance with an organic solvent to obtain a standard working solution; detecting the standard working solution by adopting a gas chromatograph, and obtaining a standard curve equation according to an external standard method; mixing a tributyrin powder sample with an organic solvent, and carrying out ultrasonic treatment and filtering treatment to obtain a to-be-detected sample solution; and detecting the to-be-detected sample solution by adopting a gas chromatograph, and obtaining the content of tributyrin in the to-be-detected sample solution according to the standard curve equation and the determined peak area. The determination method has the advantages of simplicity and convenience in operation, good repeatability, accuracy and the like, wherein the recovery rate of the tributyrin is between 98.8% and 100.2%.

The invention belongs to the technical field of feed additives, and particularly relates to a feed additive for improving meat quality of eleutheronema tetradactylum and a preparation method of the feed additive. Aiming at the problem that the meat quality of eleutheronema tetradactylum becomes poor under low salinity when the eleutheronema tetradactylum is artificially fed at present, the invention provides the feed additive for improving the meat quality of the eleutheronema tetradactylum, and the feed additive comprises the following components in percentage by weight: 5-8% of vitamin A, 12-15% of vitamin D, 6-10% of lauric acid, 8-12% of carnitine, 3-5% of manganese methionine and 5-8% of lactic acid bacteria. The feed comprises the following components in percentage by weight: 5-10% of tributyrin, 3-7% of inositol, 3-5% of magnesium aspartate, 5-8% of lysophosphatide and 12-40% of corn flour. The invention also provides a preparation method of the additive. The additive disclosed by the invention has a remarkable improvement effect on the water-holding capacity, tenderness, meat color, chewiness, flavor amino acid content and the like of eleutheronema tetradactylum muscle, can improve the meat quality of eleutheronema tetradactylum, and has a very good practical value.

The invention relates to a method for compartment analysis of ferulic acid glycerol monobutyralte through the high performance liquid chromatography, comprising the following: firstly, a step of pretreatment, during which, ferulic acids and absolute ethyl alcohols generate reflux heating reaction under the catalysis of thionyl chlorides and are dissolved in aether and then ferulic acid methyl ethyl oxalate is obtained after extraction through sodium bicarbonate; under the temperature of between 30 and 50 DEG C, tertiary butyl alcohol is used as reaction medium and the ferulic acid glycerol monobutyralte is obtained through oscillating reaction of the ferulic acid methyl ethyl oxalate, glycerol monobutyralte and Novozym435 lipase in an air bath; the ferulic acid glycerol monobutyralte is dissolved in methanol, filtered and then diluted by HPLC-level methanol; secondly, a step of compartment analysis, which is to adopt a chromatographic column (Ph-3 column Inertsil, IDx250mm) with a column temperature of ambient temperature. A solid phase adopts silica gel filler and the ultraviolet detection wavelength is between 280 and 325 nanometers; a moving phase is gradient mixing of methanoland water; the sample feeding quantity is 5 mu L and the flow speed is 1mL / min. The method selects filler of the chromatographic column and the special ultraviolet scanning wavelength according to the characteristics of materials to be comparted, is quick, high-efficient and accurate and is convenient for industrial analysis and application.

The invention relates to the field of preparation of food antioxidants, particularly to a method for synthesizing a functional food antioxidant dibutyrin ferulate. The method comprises the following steps of: performing condensation reaction on glycerol and acetone to ensure that two hydroxyl groups in the glycerol are firstly protected by the acetone, and then exposing unprotected hydroxyl groups, carrying out esterification reaction with the carboxyl of ferulic acid to graft the ferulic acid on glycerol to obtain a material B; deprotecting the protected hydroxyl in a dilute acid solution, dissociating the two hydroxyl groups, and carrying out esterification reaction on the dissociated hydroxyl groups and butyryl chloride to finally obtain the food antioxidant dibutyrin ferulate. The yield of the dibutyrin ferulate prepared by the method is high, and the preparation conditions are mild.

The invention relates to a premix capable of promoting growth and reproduction of sows, as well as a preparation method and an application thereof. In parts by weight, per 1000 parts of the premix capable of promoting growth and reproduction of the sows comprises the following ingredients: 15-30 parts of selenium yeast, 150-200 parts of glycine chelated manganese, 36-50 part of copper lysine, 0.1-0.2 part of chromium picolinate, 1-2 parts of folic acid, 20-80 parts of linseed meal, 50-200 parts of glyceryl butyrate, and the balance carriers. The premix is added into basic daily feeds of the sows in a dosage that the addition amount of the premix is 0.5-1% of the total mass of the basic daily feeds of the sows. Compared with the prior art, the premix disclosed by the invention is capable of effectively improving food intake and milk yield of the sows, as well as satisfying nutrition needs so as to ensure nutrition, healthy development and production performance of the sows and the piglets. The premix promotes growth and breeding of the sows, and improves intestinal immune functions; moreover, the premix improves lactation performance, and reduces weight and back fat loss of the sows in the lactation period. In addition, the premix satisfies macro-element and trace-element needs of the sows in the breeding cycles, as well as improves absorption and utilization rates and reduces pollution to the environment.

The invention belongs to the technical field of preparation of glyceryl monobutyrate, and discloses a distillation method for purifying glyceryl monobutyrate, which comprises the following steps: raw oil is placed in a reaction tank, air in the raw oil is removed through pretreatment, and the raw oil is obtained through esterification reaction of butyric acid and glyceryl ester; short-diameter molecular distillation equipment is adopted to purify the raw oil, the operating temperatures of a film evaporator and a molecular distiller of the short-diameter molecular distillation equipment are controlled not to exceed 95 DEG C, the raw oil is controlled to be 1-2 mL / min, and the vacuum degrees of the film evaporator and the molecular distiller are controlled to be 0-50 mmHg, so that high-purity glyceryl monobutyrate is obtained; in conclusion, based on the molecular distillation method provided by the invention, the impurities such as butyric acid, glycerol, dibutyrin and tributyrin can be effectively removed, so that the peculiar smell of the glyceryl monobutyrate can be effectively reduced, and the purity of the obtained glyceryl monobutyrate finished product is ensured to reach 90% or above.

An enzymatic method for preparing glyceryl butyrate, comprising: (1) carrying out an esterification reaction between n-butyric acid and glycerol using lipase as a catalyst, ethyl acetate and / or ethyl formate as an additive; (2) separating the reaction product, recovering the additive by distillation under reduced pressure to obtain glyceryl butyrate. The invention uses lipase as a catalyst to catalyze the esterification reaction of n-butyric acid and glycerin at normal temperature and normal pressure, reduces the energy consumption of the reaction. Also, the reaction condition is mild, no side reaction happens, and no water-carrying agent is used. In addition, the additive increases the catalytic efficiency of the lipase and the conversion rate of butyric acid.

The invention provides a feed additive for preventing and treating white feces of prawns, wherein the feed additive comprises the raw materials: tannic acid, ursolic acid and butyrin, and the mass ratio of tannic acid to ursolic acid to butyrin is calculated to be (2-4):(1-2):(2-4). The feed additive for preventing and treating white feces of prawns provided by the invention can improve the intestinal health of the prawns by improving the antioxidant capacity of prawn body tissues, effectively prevent the symptoms of white feces of litopenaeus vannamei, or effectively relieve the symptoms of white feces when white feces occurs, and reduce the probability of jejunum empty stomach and mortality of the prawns.

The invention relates to a composite feed additive for restoring baby pig intestine mucosal injury, belonging to the technical field of feed additives for baby pigs. The feed additive comprises 0.1-0.2 part of glutamine, 0.01-0.1 part of butyrin, 0.01-0.1 part of yeast nucleic acid, 0.02-0.2 part of threonine, 0.03-0.3 part of origanum oil, 0.03-0.3 part of chitooligosaccharide, 0.1-0.5 part of active dry yeast, 0.1-0.5 part of Bacillus subtilis, 0.11-0.3 part of vitamin and 5-7.5 parts of carrier. On the basis of the basic principles of baby pig intestinal tract nutrition, intestinal tract immunity and intestinal tract microecology, the invention can effectively restore baby pig intestine mucosal injury, accelerate the growth of baby pigs, and promote the health and immunity of the baby pig intestinal tract, thereby enhancing the survival rate and growth rate of the baby pigs.

The invention discloses a use of an oil and fat composition in preparing pig and poultry feed, a feed additive and a feed. Wherein, the feed additive includes glycerol monobutyrate, glycerol tricaproate, glycerol trilactate and auxiliary materials, wherein, by weight, 0.5 to 1 part of glycerol monobutyrate and 1 part of glycerol tricaproate ~ 2 parts, 1 part trilactide. The technical scheme of the invention can reduce the body fat content of pigs and poultry, increase the percentage of lean meat and poultry breast, and reduce the cost of feed additives.