An MAS probe is disclosed for obtaining a substantial improvement in 
signal to 
noise (S / N) in triple-
resonance high-resolution (HR) magic-angle-
spinning (MAS) NMR of samples near 
room temperature (RT) in high-field magnets where the 
magnet's RT shim bore is greater than 60 mm. All critical circuit components, including the sample coils, are located along with the spinner 
assembly in a thermally insulated 
cold zone pressurized with 
helium gas. The spinner 
assembly attaches to a sealed, curved, rotor-loading tube to permit automatic sample change, and it is surrounded by a partially insulated jacket cooled with a cryogenic fluid, generally 
nitrogen gas. The MAS probe is also compatible with 
magic angle gradients, variable temperature operation, field locking, and commonly available closed-cycle cold fingers. One major challenge in implementing CryoMAS is solving the problem of gas leakage from the spinner bearing, drive, and exhaust 
nitrogen into the 
cold zone, as some components will necessarily be 
ceramic, some plastic, and some 
metal. It is not desirable to use 
helium for the spinner bearing and drive gases for cost reasons and to prevent risk of degradation of o-ring-sealed 
magnet cryostats. A pressurized 
helium atmosphere in the 
cold zone may be utilized to prevent 
nitrogen flow from the spinner exhaust streams or 
atmosphere into the cold zone. The drawback to a pressurized cold zone is that the 
heat transfer coefficient in dense helium at low temperatures is very high, making it challenging to cool the sample coils and all the large, critical, circuit components in a practical manner. Part of the solution here is to use a first-stage cooling-jacket around the major heat leaks near the spinner exhaust flows. The critical components may be insulated with fine 
glass wool or teflon foam and conduction cooled without cooling much of the cold zone below the temperature of the first-stage cooling. The use of coaxial 
sapphire capacitors allows the 
noise contributions from the most critical capacitors to be reduced to a minor fraction of the total.